Binary Distillation

Model Continuous Distillation Equipment in the Industry as well as Flash & Batch Separation Processes in Binary Systems

Last updated 2022-01-10 | 4.4

- Understand the Principles behind Binary Distillation
- Design & Operate Flashing
- and Flash Drums via Flash Distillation of Binary Mixtures
- Understand and apply the principles and methods for simple distillation of binary mixtures

What you'll learn

Understand the Principles behind Binary Distillation
Design & Operate Flashing
and Flash Drums via Flash Distillation of Binary Mixtures
Understand and apply the principles and methods for simple distillation of binary mixtures
Understand Continuous Distillation Equipment
Model Distillations of Binary Systems
Apply McCabe-Thiele Method for Continuous Distillation Column Design (Number of Stages)
Simulate several process
specially continuous and batch distillation of binary mixtures
Get to know the "Recycle Ratio"
"Reboiler Duty"
"Feed Stage" etc...
Model Stripping and Enriching Sections of a Distillation Column

* Requirements

* Mass Transfer Basics
* Transport Phenomena
* Thermodynamics
* Mass and Energy Balances
* Physical Chemistry

Description

Introduction:

Binary Distillation is one of the most important Mass Transfer Operations used extensively in the Chemical industry.

Understanding the concept behind Gas-Gas, Liquid-Liquid and the Gas-Liquid mass transfer interaction will allow you to understand and model Distillation Columns, Flashes, Batch Distillator, Tray Columns and Packed column, etc...

We will cover:

  • REVIEW: Of Mass Transfer Basics (Equilibrium VLE Diagrams, Volatility, Raoult's Law, Azeotropes, etc..)

  • Distillation Theory

  • Application of Distillation in the Industry

  • Counter-Current Operation

  • Several equipment to Carry Gas-Liquid Operations

  • Bubble, Spray, Packed and Tray Column equipment

  • Flash Distillation & Flash Drums Design

  • Design & Operation of Tray Columns

  • Number of Ideal Stages: McCabe Thiele Method & Ponchon Savarit Method

  • Recycle

  • Condenser types: partial, total

  • Pressure drop due to trays

  • Design & Operation of Packed Columns

  • Pressure drop due to trays

  • Efficiency of Stages & Murphree's Efficency

  • Batch Distillation, the Raleigh Equation

  • Software Simulation for Absorption/Stripping Operations (ASPEN PLUS/HYSYS)

Solved-Problem Approach:

All theory is backed with exercises, solved problems, and proposed problems for homework/individual study.

At the end of the course:

You will be able to understand mass transfer mechanism and processes behind Binary Distillation in Flash, Continuous & Batch Processes. You will be able to continue with a Multi-Component Distillation, Reactive Distillation and Azeotropic Distillation as well as more Mass Transfer Unit Operation Courses and/or Separation Processes Course.

About your instructor:

I majored in Chemical Engineering with a minor in Industrial Engineering back in 2012.

I worked as a Process Design/Operation Engineer in INEOS Koln, mostly on the petrochemical area relating to naphtha treating. There I designed and modeled several processes relating separation of isopentane/pentane mixtures, catalytic reactors and separation processes such as distillation columns, flash separation devices and transportation of tank-trucks of product.

Who this course is for:

  • Chemical Engineers refreshing their Mass Transfer and Separation Processes course
  • Students on the relevant fields (chemical, mechanical, process engineering)
  • Engineers working with Distillation Columns / Flash Drums
  • Process Separation Engineer

Course content

5 sections • 77 lectures

Introduction to Distillation Preview 08:01

Requirements Preview 04:44

Reference Material Preview 01:31

Ideal Gas Preview 03:43

Ideal Solution Preview 05:02

Vapor Pressure Preview 04:55

Partial Pressure Preview 02:38

What is Equilibrium? (Pure Substances) Preview 03:36

Raoult’s Law Preview 05:17

What is Flux? Preview 09:05

What is Ja? Diffusion Flux Preview 02:42

Convection Preview 04:38

Type of Equipment - Dispersion of Gas-Liquid and Liquid-Gas Preview 04:12

Spray Column Preview 02:36

Bubble Column Preview 02:00

Packed Column Preview 01:32

Tray Column Preview 01:25

Types of Operation Preview 01:39

Single vs. Multiple Stage Preview 08:28

Introduction to Tray Columns Preview 04:18

Sieve Trays Preview 04:08

Valve Trays Preview 03:57

Bubble Cap Trays Preview 03:39

Tray Considerations Preview 00:27

Trays - Spacing Preview 02:28

Trays - Sizing Preview 01:12

Trays - Layouts Preview 04:48

Trays - Materials Preview 02:50

Trays - Manways Preview 01:30

Trays - Operations Preview 01:37

Tray - Pressure Drop Preview 01:27

Trays - Costs Preview 01:07

Tray - Maintenance Preview 00:53

Trays - Summary Preview 01:04

All other Pieces Preview 00:27

Bubbling Area Preview 01:43

Contact Area Preview 01:24

Weir Preview 02:34

Downcomer Preview 03:54

Stage Efficiency Preview 05:44

Murphree's Efficiency Preview 03:30

Column Operation Preview 02:51

Column Operation - Normal Preview 02:04

Column Operation - Flooding Preview 03:41

Column Operation - Priming Preview 02:26

Column Operation - Coning Preview 01:43

Column Operation - Weeping Preview 01:47

Column Operation - Dumping Preview 03:37

Column Operation - Summary Preview 03:34

Tray Diameter Introduction Preview 06:14

Tray Spacing Preview 02:25

Pressure Drop in Trays Preview 03:49

Hd, Dry Liquid sieve loss - Pressure Drop in trays Preview 03:07

Hl, (equivalent h eight of clear liquid holdup) Preview 03:39

Hd, Surface Tension Pressure loss Preview 01:17

Packed Columns vs. Tray Columns Preview 05:03

Introduction to Packings Preview 04:05

Packing Material Preview 02:26

Random Packing Preview 01:28

Stacked Packing Preview 01:39

Structural Packing Preview 00:58

Other Column Internals Preview 01:51

Liquid distributor Preview 02:13

Liquid/Vapour Re-Distributor Preview 01:07

Vapour Distributor Preview 01:12

Demister / Mist Eliminator Preview 01:45

Vortex breaker Preview 00:48

Packing Supports Preview 01:23

Retaining devices (Hold-down Plate & Bed limiter ) Preview 01:07

Column Structure - Top Preview 01:23

Column Structure - Middle Preview 01:44

Column Structure - Bottom Preview 10:33

Benzene and toluene Feed Tray, Min. Recycle Ratio, etc Preview 06:55

WKS RadFrac - C3 - iC4 Separation - Recycle Preview 05:08

WKS RadFrac - Column Internals, Trays vs Packings Preview 11:28

WKS Sensitivity Analysis of Feed Stages, Reflux Ratios and Pressure in a RadFrac Preview 10:30